Issue 41, 2020
From the journal:

Organic & Biomolecular Chemistry

Radical cyclizations of enynes/dienes with alcohols in water using a green oxidant†

Dong-Kai Wang,‡a   Yi-Lin Fang,‡bc   Jian Zhang,a   Yu-Tao Guan,a   Xun-Jie Huang,a   Jianfeng Zhang,*a   Qiang Li ORCID logo *b  and  Wen-Ting Wei ORCID logo *a  

* Corresponding authors

a State Key Laboratory Base of Novel Functional Materials and Preparation Science, School of Materials Science and Chemical Engineering, Ningbo University, Ningbo, Zhejiang, China
E-mail: zhangjianfeng1@nbu.edu.cn, weiwenting@nbu.edu.cn

b Institution of Functional Organic Molecules and Materials, School of Chemistry and Chemical Engineering, Liaocheng University, Liaocheng 252059, China
E-mail: tiamochem@hotmail.com

c Department of Chemistry, Guilin Normal College, Gulin 541199, China

Abstract

A simple, eco-friendly, and efficient methodology for performing radical cyclizations of enynes/dienes with alcohols in water has been established. This methodology showed ease of scale up, and it was designed to use mild reaction conditions and no catalyst. It was also designed to employ K2S2O8 as a green oxidant and water as the solvent, conditions making this process clean and easy to operate, hence achieving the criteria of green chemistry.

Graphical abstract: Radical cyclizations of enynes/dienes with alcohols in water using a green oxidant

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Article information

DOI
https://doi.org/10.1039/D0OB01902J
Article type
Paper
Submitted
16 Sep 2020
Accepted
05 Oct 2020
First published
06 Oct 2020

Org. Biomol. Chem., 2020,18, 8491-8495

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Radical cyclizations of enynes/dienes with alcohols in water using a green oxidant

D. Wang, Y. Fang, J. Zhang, Y. Guan, X. Huang, J. Zhang, Q. Li and W. Wei, Org. Biomol. Chem., 2020, 18, 8491 DOI: 10.1039/D0OB01902J

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