Azobenzene-based unnatural amino acid scaffolds via a Pd(II)-catalyzed C(sp3)–H arylation strategy

Radha Tomar; Sonam Suwasia; Angshuman Roy Choudhury; Sugumar Venkataramani; Srinivasarao Arulananda Babu

doi:10.1039/D2CC04870A

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Azobenzene-based unnatural amino acid scaffolds via a Pd(ii)-catalyzed C(sp³)–H arylation strategy†

Radha Tomar,‡^a Sonam Suwasia,‡^a Angshuman Roy Choudhury,

^a Sugumar Venkataramani

*^a and Srinivasarao Arulananda Babu

*^a

Author affiliations

* Corresponding authors

^a Department of Chemical Sciences, Indian Institute of Science Education and Research (IISER) Mohali, Knowledge City, Sector 81, SAS Nagar, Manauli P.O. 140306, Mohali, Punjab, India
E-mail: sugumarv@iisermohali.ac.in, sababu@iisermohali.ac.in

Abstract

Azobenzene-based unnatural amino acid motifs were synthesized via Pd(II)-catalyzed diastereoselective C(sp³)–H arylation of amino acid carboxamides with iodoacetanilides and Mills azo coupling.

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Article information

DOI: https://doi.org/10.1039/D2CC04870A
Article type: Communication
Submitted: 02 Sep 2022
Accepted: 26 Oct 2022
First published: 26 Oct 2022

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Chem. Commun., 2022,58, 12967-12970

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Azobenzene-based unnatural amino acid scaffolds via a Pd(II)-catalyzed C(sp³)–H arylation strategy

R. Tomar, S. Suwasia, A. R. Choudhury, S. Venkataramani and S. A. Babu, Chem. Commun., 2022, 58, 12967 DOI: 10.1039/D2CC04870A

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