The unprecedented samarium electrocatalyzed reductive alkoxylation of phthalimides in a single step is presented. Under mild conditions, using electrogenerated Sm(II) with TMSCl (trimethyl chlorosilane), N-substituted 3-alkoxyl isoindolin-1-ones are isolated in good to excellent yields with high functional group tolerance.
Y. Zhang and M. Mellah, Org. Chem. Front., 2022, 9, 1308 DOI: 10.1039/D1QO01760H
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