We synthesized Li and Na monocarborate salts with minimal protic impurities and reassessed their electrochemical windows. Na salts display higher efficiency for metal deposition/stripping and are more oxidatively stable than Li salts. This strong cation effect is rationalized in terms of differences in charge density between Li+ and Na+ cations.
O. Tutusaus, H. Kuwata, M. J. Counihan and R. Mohtadi, Chem. Commun., 2023, 59, 4746 DOI: 10.1039/D2CC06938E
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