Enhanced Li-ion conductivity in LiBH4–ZrO2 nanocomposites and nanoscale Li imaging by energy-filtered transmission electron microscopy

Yuki Nakagawa; Tsubasa Sendo; Tamaki Shibayama

doi:10.1039/D3CC02860G

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Enhanced Li-ion conductivity in LiBH₄–ZrO₂ nanocomposites and nanoscale Li imaging by energy-filtered transmission electron microscopy†

Yuki Nakagawa,

*^a Tsubasa Sendo^b and Tamaki Shibayama

Author affiliations

* Corresponding authors

^a Faculty of Engineering, Hokkaido University, N-13, W-8, Sapporo 060-8628, Japan
E-mail: y-nakagawa@eng.hokudai.ac.jp

^b Graduate School of Engineering, Hokkaido University, N-13, W-8, Sapporo 060-8628, Japan

Abstract

A complementary solid-state nuclear magnetic resonance and transmission electron microscopy (TEM) analysis was performed for LiBH₄–ZrO₂ nanocomposites. As a result, amorphous LiBH₄ films with thicknesses of less than 30 nm were observed covering the ZrO₂ particles. Li imaging by energy-filtered TEM is useful for the real-space characterization of nanoscale LiBH₄.

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Article information

DOI: https://doi.org/10.1039/D3CC02860G
Article type: Communication
Submitted: 14 Jun 2023
Accepted: 11 Aug 2023
First published: 15 Aug 2023

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Chem. Commun., 2023,59, 10912-10915

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Enhanced Li-ion conductivity in LiBH₄–ZrO₂ nanocomposites and nanoscale Li imaging by energy-filtered transmission electron microscopy

Y. Nakagawa, T. Sendo and T. Shibayama, Chem. Commun., 2023, 59, 10912 DOI: 10.1039/D3CC02860G

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Chemical Communications