One-pot synthesis of structurally diverse sulfurized/selenated 4-aminopyrimidines has been reported via t-BuOK/K2S2O8-promoted four-component reaction of mixed nitriles and disulfides/diselenides. Mechanistic studies indicate that the reaction proceeds through radical and ionic pathways, and an alkenyl sulfide serves as a key intermediate.
H. Wang, Y. Zhu, C. Chen, X. Huang, M. Liu, Y. Zhou and H. Wu, Chem. Commun., 2024, 60, 862 DOI: 10.1039/D3CC05416K
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