Guanidinium organosulfonate (GS) hydrogen-bonded host frameworks were used to trap α-halopropiophenones and α-halocyclooctanones to determine their molecular structure by single crystal X-ray diffraction. The majority of encapsulated guest molecules adopted conformations expected from computational analysis and stereochemical outcomes of Grignard reactions.
A. M. Dillon, A. G. Shtukenberg, K. M. Demkiw, K. A. Woerpel and M. D. Ward, Chem. Commun., 2024, 60, 11770 DOI: 10.1039/D4CC03430A
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