Tropic acid was synthesized in a good yield and with high enantioselectivity (81% ee) under non-biphasic conditions via the novel hydrolytic dynamic kinetic resolution of racemic 3-phenyl-2-oxetanone (tropic acid β-lactone) in the presence of a chiral quaternary ammonium phase-transfer catalyst and strongly basic anion exchange resin as the hydroxide ion donor.
M. Kawasaki, T. Shirai, K. Yatsuzuka and R. Shirai, RSC Adv., 2024, 14, 6121 DOI: 10.1039/D3RA08594E
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