Both the B–S and S–S bonds of 1,2,4,3,5-trithiadiborolane 1 could be cleaved by potassium graphite (KC8) to give the first isolable boryl dithiolate DmpB(SK)23, whereas the reduction of 1,2,4-triselena-3,5-diborolane 2 with KC8 afforded the boryl diselenolate DmpB(SeK)(SeSeK) 4, showcasing the unprecedented structural authentication of ligand substituted diselenolate.
Y. Dai, Y. Wang, L. Wang, F. Qi, Q. Li and L. Kong, Chem. Commun., 2025, 61, 169 DOI: 10.1039/D4CC05240D
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