Using zinc (0) in a 5% v AcOH aqueous solution allowed the efficient pinacol coupling of aliphatic or aromatic unusual, α,β-unsaturated carbonyl compounds such as citral A in good to excellent yields (56–99%). It can also be successfully applied to acetophenone.
M. Billamboz, N. Sotto, C. Chevrin-Villette and C. Len, RSC Adv., 2015, 5, 46026 DOI: 10.1039/C5RA03870G
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