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The microwave synthesis of two prototypical porous organic cages, denoted as CC3 and CC2, is demonstrated. CC3 crystals displaying a narrow size distribution were synthesized in just a few minutes. The fast synthesis of narrow size distribution POC crystals makes microwave synthesis a highly appealing approach for the synthesis of these crystals.

Graphical abstract: Microwave-assisted synthesis of porous organic cages CC3 and CC2

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