Xiaopeng
Zhang
*,
Qianqian
Ding
,
Jinjun
Wang
,
Jingyi
Yang
,
Xuesen
Fan
and
Guisheng
Zhang
*
Key Laboratory of Green Chemical Media and Reactions, Ministry of Education, Collaborative Innovation Center of Henan Province for Green Manufacturing of Fine Chemicals, Henan Key Laboratory of Organic Functional Molecule and Drug Innovation, School of Chemistry and Chemical Engineering, Henan Normal University, Xinxiang 453007, China. E-mail: 031128@htu.edu.cn; zgs@htu.cn
First published on 8th January 2021
Correction for ‘Pd(II)-Catalyzed [4 + 1 + 1] cycloaddition of simple o-aminobenzoic acids, CO and amines: direct and versatile synthesis of diverse N-substituted quinazoline-2,4(1H,3H)-diones’ by Xiaopeng Zhang et al., Green Chem., 2021, DOI: 10.1039/d0gc03254a.
Entry | T (°C) | Additive | Oxidant | Solvent | Y (%) |
---|---|---|---|---|---|
a Reaction conditions: 1b (1.0 mmol), 2a (3.0 mmol), KI (0.2 mmol), Cu(OAc)2 (1.0 mmol), solvent (10 mL); 2a (and 1.0 mmol AcOH) was added 6 h later. b Isolated yields. c CO:O2 = 5:1. d The mixture of 2a and AcOH (1.0 mmol) was added dropwise. | |||||
1c | 30 | KI/AcOH | Cu(OAc)2/O2 | CH3CN | 53 |
2c | 40 | KI/AcOH | Cu(OAc)2/O2 | CH3CN | 71 |
3c | 60 | KI/AcOH | Cu(OAc)2/O2 | CH3CN | 81 |
4c | 70 | KI/AcOH | Cu(OAc)2/O2 | CH3CN | 80 |
5d | 60 | KI/AcOH | Cu(OAc)2/O2 | CH3CN | 55 |
6 | 60 | KI/AcOH | Cu(OAc)2 | CH3CN | 85 |
7 | 60 | KI | Cu(OAc)2 | CH3CN | 85 |
8 | 60 | KI | Cu(OAc)2 | Toluene | Trace |
9 | 60 | KI | Cu(OAc)2 | DMSO | ND |
10 | 60 | KI | Cu(OAc)2 | DMF | ND |
11 | 60 | KI | Cu(OAc)2 | 1,4-Dioxane | ND |
The Royal Society of Chemistry apologises for these errors and any consequent inconvenience to authors and readers.
This journal is © The Royal Society of Chemistry 2021 |