Issue 34, 2023
From the journal:

Chemical Communications

Direct observation of crystal degradation behaviour in porous crystals under low-dose electron diffraction conditions†

Hikaru Sakamotoa  and  Masataka Ohtani ORCID logo *a  

* Corresponding authors

a School of Environmental Science and Engineering, Kochi University of Technology, 185 Miyanokuchi, Tosayamada, Kami, Kochi 782-8502, Japan
E-mail: ohtani.masataka@kochi-tech.ac.jp

Abstract

The quantification of electron beam damage in crystalline porous materials has been investigated under low-dose electron irradiation conditions. As a result of the systematic quantitative analysis of time-course changes in electron diffraction patterns, it was found that the unoccupied volume in the MOF crystal is a crucial factor for electron beam resistance.

Graphical abstract: Direct observation of crystal degradation behaviour in porous crystals under low-dose electron diffraction conditions

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Article information

DOI
https://doi.org/10.1039/D3CC00506B
Article type
Communication
Submitted
03 Feb 2023
Accepted
29 Mar 2023
First published
29 Mar 2023

Chem. Commun., 2023,59, 5039-5042

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Direct observation of crystal degradation behaviour in porous crystals under low-dose electron diffraction conditions

H. Sakamoto and M. Ohtani, Chem. Commun., 2023, 59, 5039 DOI: 10.1039/D3CC00506B

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