1-Amino-o-carbaborane anions, (o-RCB10H10CNH2)2– in liquid NH3 have been found to be oxidized with KMnO4 to give the symmetrically substituted 1-azo-o-carbaboranes, RCB10H10CN![[double bond, length half m-dash]](https://www.rsc.org/images/entities/char_e006.gif)
NCB10H10CR (R = H, Me, Ph).
T. Totani, K. Aono, H. Nakai and M. Shiro, J. Chem. Soc., Chem. Commun., 1979, 1051 DOI: 10.1039/C39790001051
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