Ruthenium redox couples have been immobilized on the perpendicular surface of poly sulphur nitride (SN)x, single-crystals which were used as electrodes and which, when maintained at about –0·10 V vs the saturated calomel electrode in H2SO4 solution and illuminated with visible light, evolve hydrogen gas continuously.
H. B. Mark, A. Voulgaropoulos and C. A. Meyer, J. Chem. Soc., Chem. Commun., 1981, 1021 DOI: 10.1039/C39810001021
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