Molybdenum-doped tin(IV) oxide has been shown by electron microscopy to contain many planar defects including twin boundaries; the segregation of molybdenum to these twin boundaries has been unequivocally established by X-ray microanalysis and associated with the thermally induced migration of molybdenum to more favourable sites within the rutile-type lattice.
F. J. Berry, C. Hallett, M. H. Loretto and D. J. Smith, J. Chem. Soc., Chem. Commun., 1984, 1483 DOI: 10.1039/C39840001483
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