The thermolysis of [2.2.2]paracyclophane in the presence of an excess of [Co4(CO)12] yields three new arene clusters [{Co4(CO)9}n(C24H24)] (n = 1, 2 and 3): the molecular structures of the mono- and bis-cluster complexes have been established by single crystal X-ray diffraction while the tris-complex has been characterised by spectroscopy.
P. Schooler, B. F. G. Johnson, C. M. Martin, P. Schooler, C. M. Martin, P. J. Dyson and S. Parsons, Chem. Commun., 1998, 795 DOI: 10.1039/A800715B
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