Solutions of sodium benzeneselenolate sufficiently reactive to effect aromatic substitution and ester dealkylation are prepared in DMSO or NMP from diphenyl diselenide and hydrazine hydrate by titration with methanolic sodium methanolate.
L. Henriksen and N. Stuhr-Hansen, J. Chem. Soc., Perkin Trans. 1, 1999, 1915 DOI: 10.1039/A903686E
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