Total synthesis of new C-6 homologues of1-deoxynojirimycin and 1-deoxy-L-idonojirimycin

Peter Szolcsányi; Tibor Gracza; Marian Koman; Naïa Prónayová; Tibor Liptaj

doi:10.1039/A908449E

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Total synthesis of new C-6 homologues of 1-deoxynojirimycin and 1-deoxy-l-idonojirimycinPart of PhD Thesis of P. S. E-mail: szol@chelin.chtf.stuba.sk

Peter Szolcsányi,^a Tibor Gracza,*^a Marian Koman,^b Naïa Prónayová^c and Tibor Liptaj^c

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* Corresponding authors

^a Department of Organic Chemistry, Faculty of Chemical Technology, Slovak University of Technology, Radlinského 9, Bratislava, Slovakia.
E-mail: gracza@chelin.chtf.stuba.sk

^b Department of Inorganic Chemistry, Faculty of Chemical Technology, Slovak University of Technology, Radlinského 9, Bratislava, Slovakia

^c Central NMR Laboratories, Faculty of Chemical Technology, Slovak University of Technology, Radlinského 9, Bratislava, Slovakia

Abstract

Novel piperidine lactones 1 and 2, which represent direct precursors to the new C-6 homologues of 1-deoxynojirimycin (3) and 1-deoxy-L-idonojirimycin 4, were prepared by key Pd^II-catalysed aminocarbonylation of protected aminoalkene 10.

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Article information

DOI: https://doi.org/10.1039/A908449E
Article type: Communication
Submitted: 21 Oct 1999
Accepted: 25 Jan 2000
First published: 02 Mar 2000

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Chem. Commun., 2000, 471-472

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Total synthesis of new C-6 homologues of 1-deoxynojirimycin and 1-deoxy-L-idonojirimycin

P. Szolcsányi, T. Gracza, M. Koman, N. Prónayová and T. Liptaj, Chem. Commun., 2000, 471 DOI: 10.1039/A908449E

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