Issue 2, 2005
From the journal:

Chemical Communications

Highlighting gyroscopic motion in crystals in 13C CPMAS spectra by specific isotopic substitution and restricted cross polarization

Steven D. Karlena  and  Miguel A. Garcia-Garibay*a  

* Corresponding authors

a Department of Chemistry and Biochemistry, University of California, Los Angeles, California, USA
E-mail: mgg@chem.ucla.edu

Abstract

The temperature-dependent exchange rate and signal coalescence in the 13C CPMAS NMR spectrum of a crystalline molecular gyroscope are exposed by specifically deuterating the overlapping static carbons.

Graphical abstract: Highlighting gyroscopic motion in crystals in 13C CPMAS spectra by specific isotopic substitution and restricted cross polarization

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Article information

DOI
https://doi.org/10.1039/B409744K
Article type
Communication
Submitted
26 Jun 2004
Accepted
21 Sep 2004
First published
24 Nov 2004

Chem. Commun., 2005, 189-191

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Highlighting gyroscopic motion in crystals in 13C CPMAS spectra by specific isotopic substitution and restricted cross polarization

S. D. Karlen and M. A. Garcia-Garibay, Chem. Commun., 2005, 189 DOI: 10.1039/B409744K

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