Issue 48, 2009
From the journal:

Chemical Communications

In situneutron powder diffraction and structure determination in controlled humidities†

Valeska P. Ting,a   Paul F. Henry,b   Marc Schmidtmann,c   Chick C. Wilsonc  and  Mark T. Weller*a  

* Corresponding authors

a School of Chemistry, University of Southampton, UK
E-mail: mtw@soton.ac.uk
Fax: +44 (0)23 8059 33781
Tel: +44 (0)23 8059 3592

b MI-1, Helmholtz Zentrum Berlin für Materialien und Energie, Berlin, Germany
E-mail: paul.henry@helmholtz-berlin.de
Tel: +49 30 8062 2686

c WestCHEM, Department of Chemistry, University of Glasgow, UK
E-mail: c.c.wilson@chem.gla.ac.uk
Fax: +44 (0)141 330 8522

Abstract

A controlled-humidity sample environment has been constructed, allowing bulk powder samples undergoing humidity-induced phase transitions and reactions to be studied via in situ neutron diffraction. Associated developments in data collection and analysis permit this to be achieved without the use of D2O.

Graphical abstract: In situ neutron powder diffraction and structure determination in controlled humidities

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Article information

DOI
https://doi.org/10.1039/B918702B
Article type
Communication
Submitted
09 Sep 2009
Accepted
20 Oct 2009
First published
05 Nov 2009

Chem. Commun., 2009, 7527-7529

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In situ neutron powder diffraction and structure determination in controlled humidities

V. P. Ting, P. F. Henry, M. Schmidtmann, C. C. Wilson and M. T. Weller, Chem. Commun., 2009, 7527 DOI: 10.1039/B918702B

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