Issue 1, 2009
From the journal:

CrystEngComm

Increased control over the desolvation of p-tert-butylcalix[5]arene†

Jian Tian,a   Scott J. Dalgarno,ab   Praveen K. Thallapally‡a  and  Jerry L. Atwood*a  

* Corresponding authors

a Department of Chemistry, University of Missouri-Columbia, 601 S. College Avenue, Columbia, USA
E-mail: AtwoodJ@missouri.edu
Fax: +1 573 882 2754
Tel: +1 573 882 8374

b School of Engineering and Physical Sciences-Chemistry, Heriot-Watt University, Edinburgh, UK

Abstract

Parital de-solvation of the toluene solvate of p-tert-butylcalix[5]arene affords a frustrated organic solid that is a new type of sorbant. Increased control over this sorption is achieved by employing a high boiling solvent for incremental de-solvation, revealing the calixarene : solvent ratio for maximum gas sorption.

Graphical abstract: Increased control over the desolvation of p-tert-butylcalix[5]arene

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Article information

DOI
https://doi.org/10.1039/B813628A
Article type
Communication
Submitted
05 Aug 2008
Accepted
18 Aug 2008
First published
15 Oct 2008

CrystEngComm, 2009,11, 33-35

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Increased control over the desolvation of p-tert-butylcalix[5]arene

J. Tian, S. J. Dalgarno, P. K. Thallapally and J. L. Atwood, CrystEngComm, 2009, 11, 33 DOI: 10.1039/B813628A

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