Synthesis and crystal structure of two new heterometallic thioantimonates(III) [Ni(pda)2]CuI4SbIII2S6 and [Ni(dien)2]CuISbIII3S6,

Meng Zhang; Tianlu Sheng; Xin Wang; Shengmin Hu; Ruibiao Fu; Jianshan Chen; Yimin He; Zhentao Qin; Chaojun Shen; Xintao Wu

doi:10.1039/B906640C

Synthesis and crystal structure of two new heterometallic thioantimonates(III) [Ni(pda)₂]Cu^I₄Sb^III₂S₆ and [Ni(dien)₂]Cu^ISb^III₃S₆†,‡

Meng Zhang,^ab Tianlu Sheng,^a Xin Wang,^a Shengmin Hu,^a Ruibiao Fu,^a Jianshan Chen,^a Yimin He,^a Zhentao Qin,^a Chaojun Shen^a and Xintao Wu*^a

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^a State Key Laboratory of Structural Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, China
E-mail: wxt@fjirsm.ac.cn.
Fax: +86-591-83714946
Tel: +86-591-83719238

^b Graduate University of the Chinese Academy of Sciences, Beijing, China

Abstract

Two different dimensional inorganic–organic hybrid heterometallic sulfide, [Ni(pda)₂]Cu₄Sb₂S₆ (1) and [Ni(dien)₂]CuSb₃S₆ (2) were obtained by using 1,2-propanediamine (pda) and diethylenetriamine (dien) as the ligand, respectively.

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Synthesis and crystal structure of two new heterometallic thioantimonates(III) [Ni(pda)₂]Cu^I₄Sb^III₂S₆ and [Ni(dien)₂]Cu^ISb^III₃S₆†,‡

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Synthesis and crystal structure of two new heterometallic thioantimonates(III) [Ni(pda)₂]Cu^I₄Sb^III₂S₆ and [Ni(dien)₂]Cu^ISb^III₃S₆,

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