Sterically congested, hexameric tetrakispyridinyl-PdII/CdII-metallomacrocycles: self-assembly and structural characterization

Sujith Perera; Xiaopeng Li; Mingming Guo; Chrys Wesdemiotis; Charles N. Moorefield; George R. Newkome

doi:10.1039/C1CC10649J

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Sterically congested, hexameric tetrakispyridinyl-Pd^II/Cd^II-metallomacrocycles: self-assembly and structural characterization†

Sujith Perera,^a Xiaopeng Li,^b Mingming Guo,^a Chrys Wesdemiotis,*^ab Charles N. Moorefield^a and George R. Newkome*^ab

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* Corresponding authors

^a Department of Polymer Science, The University of Akron, Akron, OH 44325-4717, USA
E-mail: newkome@uakron.edu, wesdemiotis@uakron.edu
Fax: +1 330-972-2413
Tel: +1 330-972-6458

^b Department of Chemistry, The University of Akron, Akron, OH 44325-3601, USA

Abstract

Hexagonal Pd^II- or Cd^II-tetrakispyridinyl-based macrocycles are quantitatively self-assembled from 4′-(3-pyridinyl)-4,4′′-di(tert-butyl)-2,2′ : 6′,2′′-terpyridine and structurally confirmed by NMR and TWIM-MS.

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Article information

DOI: https://doi.org/10.1039/C1CC10649J
Article type: Communication
Submitted: 01 Feb 2011
Accepted: 23 Feb 2011
First published: 17 Mar 2011

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Chem. Commun., 2011,47, 4658-4660

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Sterically congested, hexameric tetrakispyridinyl-Pd^II/Cd^II-metallomacrocycles: self-assembly and structural characterization

S. Perera, X. Li, M. Guo, C. Wesdemiotis, C. N. Moorefield and G. R. Newkome, Chem. Commun., 2011, 47, 4658 DOI: 10.1039/C1CC10649J

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