Issue 4, 2011
From the journal:

Green Chemistry

Organic reaction in Solkane® 365 mfc: homocoupling reaction of terminal alkynes†

Akihiro Kusuda,a   Xiu-Hua Xu,a   Xin Wang,a   Etsuko Tokunagaa  and  Norio Shibata*a  

* Corresponding authors

a Department of Frontier Materials, Graduate School of Engineering, Nagoya Institute of Technology, Gokiso, Showa-ku, Nagoya, Japan
E-mail: nozshiba@nitech.ac.jp
Fax: +81 52-735-5442

Abstract

Solkane® 365 mfc is proven to be an environmentally benign alternative solvent for the homocoupling reaction of terminal alkynes catalyzed by CuCl/TMEDA under air at room temperature. A variety of terminal alkynes, including aromatic, heteroaromatic and aliphatic alkynes, were cleanly transformed into 1,3-diynes within a short period in high to excellent yields up to 98%.

Graphical abstract: Organic reaction in Solkane® 365 mfc: homocoupling reaction of terminal alkynes

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Article information

DOI
https://doi.org/10.1039/C1GC15106A
Article type
Communication
Submitted
26 Jan 2011
Accepted
21 Feb 2011
First published
11 Mar 2011

Green Chem., 2011,13, 843-846

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Organic reaction in Solkane® 365 mfc: homocoupling reaction of terminal alkynes

A. Kusuda, X. Xu, X. Wang, E. Tokunaga and N. Shibata, Green Chem., 2011, 13, 843 DOI: 10.1039/C1GC15106A

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