Issue 46, 2012
From the journal:

Chemical Communications

Facile self-assembly of the first diphosphametacyclophane†

Amy J. Saunders,a   Ian R. Crossley,*a   Martyn P. Coles‡a  and  S. Mark Roea  

* Corresponding authors

a Department of Chemistry, University of Sussex, Brighton, UK
E-mail: i.crossley@sussex.ac.uk
Fax: +44 1273 876687
Tel: +44 1273 877302

Abstract

The reaction of isophthaloyl chloride and methyl-bis(trimethylsilyl)phosphane under mild conditions affords high yields of m-{-C(O)-C6H4(C(O)PMe)}2 (1,10-dimethyl-1,10-diphospha-[3.3]-metacyclophane-2,9,11,18-tetraone): the first example of a diphosphametacyclophane.

Graphical abstract: Facile self-assembly of the first diphosphametacyclophane

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Article information

DOI
https://doi.org/10.1039/C2CC32247A
Article type
Communication
Submitted
28 Mar 2012
Accepted
17 Apr 2012
First published
17 Apr 2012

Chem. Commun., 2012,48, 5766-5768

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Facile self-assembly of the first diphosphametacyclophane

A. J. Saunders, I. R. Crossley, M. P. Coles and S. M. Roe, Chem. Commun., 2012, 48, 5766 DOI: 10.1039/C2CC32247A

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