Issue 96, 2012
From the journal:

Chemical Communications

Poly(ethylene glycol) as reaction medium for mild Mizoroki–Heck reaction in a ball-mill†

Valérie Declerck,‡a   Evelina Colacino,a   Xavier Bantreil,a   Jean Martineza  and  Frédéric Lamaty*a  

* Corresponding authors

a Institut des Biomolécules Max Mousseron (IBMM), CNRS-Universités Montpellier 1 et 2, Place Eugène Bataillon, 34095 Montpellier Cedex 5, France
E-mail: frederic.lamaty@univ-montp2.fr
Fax: +33 (0)4 67 14 48 66

Abstract

Phosphine-free palladium-catalyzed Mizoroki–Heck reaction was performed using ball-milling in polyethylene glycol under mild conditions. Good to excellent yields of coupling products were obtained. This activation technique also allowed the concomitant formation of round shaped Pd–PEG nanoparticles that were characterized by TEM analysis.

Graphical abstract: Poly(ethylene glycol) as reaction medium for mild Mizoroki–Heck reaction in a ball-mill

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Article information

DOI
https://doi.org/10.1039/C2CC36286D
Article type
Communication
Submitted
29 Aug 2012
Accepted
16 Oct 2012
First published
16 Oct 2012

Chem. Commun., 2012,48, 11778-11780

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Poly(ethylene glycol) as reaction medium for mild Mizoroki–Heck reaction in a ball-mill

V. Declerck, E. Colacino, X. Bantreil, J. Martinez and F. Lamaty, Chem. Commun., 2012, 48, 11778 DOI: 10.1039/C2CC36286D

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