Issue 1, 2013
From the journal:

Chemical Communications

Synthesis of borasiloxane-based macrocycles by multicomponent condensation reactions in solution or in a ball mill†‡

Mirela Pascu,a   Albert Ruggi,a   Rosario Scopellitia  and  Kay Severin*a  

* Corresponding authors

a Institut des Sciences et Ingénierie Chimiques, École Polytechnique Fédérale de Lausanne (EPFL), Lausanne, Switzerland
E-mail: kay.severin@epfl.ch
Fax: +41 (0)21 6939305
Tel: +41 (0)21 6939302

Abstract

Large macrocycles containing imine and borasiloxane links are obtained in polycondensation reactions of 4-formylbenzeneboronic acid, t-Bu2Si(OH)2, and diamines. The multicomponent reactions can be performed in solution or – advantageously – by mechanochemical syntheses in a ball mill.

Graphical abstract: Synthesis of borasiloxane-based macrocycles by multicomponent condensation reactions in solution or in a ball mill

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Article information

DOI
https://doi.org/10.1039/C2CC37538A
Article type
Communication
Submitted
16 Oct 2012
Accepted
08 Nov 2012
First published
19 Nov 2012

Chem. Commun., 2013,49, 45-47

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Synthesis of borasiloxane-based macrocycles by multicomponent condensation reactions in solution or in a ball mill

M. Pascu, A. Ruggi, R. Scopelliti and K. Severin, Chem. Commun., 2013, 49, 45 DOI: 10.1039/C2CC37538A

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