X-ray crystallography showcases the distinct self-association and hydrogen-bonding patterns of organic silanediols, R2Si(OH)2, with bifunctional heterocycles for supramolecular assembly. Diffusion-ordered spectroscopy (DOSY) studies identify the dominant hydrogen-bonding patterns and structures in solution, which correlate with solid-state patterns at high concentrations.
N. T. Tran, S. O. Wilson and A. K. Franz, Chem. Commun., 2014, 50, 3738 DOI: 10.1039/C4CC00672K
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