Issue 74, 2014
From the journal:

Chemical Communications

Facile synthesis of ultra-small rhenium nanoparticles†

Tuğçe Ayvalı,ab   Pierre Lecante,c   Pier-Francesco Fazzini,d   Angélique Gillet,d   Karine Philippot*ab  and  Bruno Chaudret*d  

* Corresponding authors

a Laboratoire de Chimie de Coordination, CNRS, LCC, 205 Route de Narbonne, F-31077 Toulouse, France
E-mail: karine.philippot@lcc-toulouse.fr
Tel: +33 (0)561333182

b Université de Toulouse, UPS, INPT, LCC, F-31077 Toulouse, France

c CNRS UPR 8011, CEMES (Centre d'Elaboration des Matériaux et d'Etudes Structurales), 29 Rue Jeanne Marvig, F-31055 Toulouse, France

d LPCNO, Laboratoire de Physique et Chimie des Nano-Objets, UMR 5215 INSA-CNRS-UPS, Institut des Sciences Appliquées, 135 Avenue de Rangueil, F-31077 Toulouse, France
E-mail: chaudret@insa-toulouse.fr
Tel: +33 (0)561559655

Abstract

Ultra-small monodisperse rhenium nanoparticles (Re NPs; ca. 1.0–1.2 nm) were easily prepared by reducing the organometallic complex [Re2(C3H5)4] under a dihydrogen atmosphere under mild reaction conditions (3 bar H2; 120 °C). The particles can be stabilized by a ligand, hexadecylamine, or a polymer, polyvinylpyrrolidone and accommodate surface hydrides.

Graphical abstract: Facile synthesis of ultra-small rhenium nanoparticles

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Article information

DOI
https://doi.org/10.1039/C4CC04816D
Article type
Communication
Submitted
24 Jun 2014
Accepted
23 Jul 2014
First published
24 Jul 2014

Chem. Commun., 2014,50, 10809-10811

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Facile synthesis of ultra-small rhenium nanoparticles

T. Ayvalı, P. Lecante, P. Fazzini, A. Gillet, K. Philippot and B. Chaudret, Chem. Commun., 2014, 50, 10809 DOI: 10.1039/C4CC04816D

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