Proof-of-principle direct double cyclisation of a linear C15-precursor to a dibrominated bicyclic medium-ring ether relevant to Laurencia species

D. Christopher Braddock; Dan-Tiberiu Sbircea

doi:10.1039/C4CC06402J

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Proof-of-principle direct double cyclisation of a linear C₁₅-precursor to a dibrominated bicyclic medium-ring ether relevant to Laurencia species†

D. Christopher Braddock*^a and Dan-Tiberiu Sbircea^a

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* Corresponding authors

^a Department of Chemistry, Imperial College London, London, SW7 2AZ, UK
E-mail: c.braddock@imperial.ac.uk
Fax: +44 (0)2075945805
Tel: +44 (0)2075945772

Abstract

Bicyclic dibrominated C₁₅ medium-ring ether hexahydrolaureoxanyne was produced directly from an acyclic model C₁₅-epoxide when treated with NBS with water as the solvent.

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Article information

DOI: https://doi.org/10.1039/C4CC06402J
Article type: Communication
Submitted: 15 Aug 2014
Accepted: 01 Sep 2014
First published: 01 Sep 2014
This article is Open Access

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Chem. Commun., 2014,50, 12691-12693

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Proof-of-principle direct double cyclisation of a linear C₁₅-precursor to a dibrominated bicyclic medium-ring ether relevant to Laurencia species

D. C. Braddock and D. Sbircea, Chem. Commun., 2014, 50, 12691 DOI: 10.1039/C4CC06402J

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Chemical Communications