An efficient procedure for preparing enantiopure polycyclic ethers is reported. The protocol is based on the photo-oxidation/conjugate addition sequence over a chiral functionalized furan, which was prepared from commercially available tri-O-acetyl-D-glucal. The Michael addition step afforded two products with the same absolute configuration from a mixture of diastereomers.
G. Pazos, M. Pérez, Z. Gándara, G. Gómez and Y. Fall, Org. Biomol. Chem., 2014, 12, 7750 DOI: 10.1039/C4OB01439A
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