Issue 101, 2014
From the journal:

RSC Advances

Thermal stability of p-dimethylaminophenylpentazole†

Yu-zhang Yang,a   Yu-chuan Li,a   Ru-bo Zhang,b   Cheng-hui Suna  and  Si-ping Pang*a  

* Corresponding authors

a School of Material Science & Engineering, Beijing Institute of Technology, South Street No. 5, Zhongguancun, Haidian District, 100081 Beijing, China
E-mail: pangsp@bit.edu.cn
Web: http://pnc.bit.edu.cn/

b School of Chemistry, Beijing Institute of Technology, South Street No. 5, Zhongguancun, Haidian District, 100081 Beijing, China

Abstract

The thermal stability of p-dimethylaminophenylpentazole (1) in the solid phase has been thoroughly investigated. The decomposition process of 1 has been verified by a combination of differential scanning calorimetry (DSC), thin-layer chromatography (TLC), temperature-programmed FTIR, and Raman spectroscopy. FTIR and Raman spectra were also calculated to corroborate the results. It was found that 1 could be handled below 20 °C without any obvious deterioration, but it decomposed sharply at 56 °C. The calculated FTIR and Raman vibrational frequencies were in accord with the experimental values.

Graphical abstract: Thermal stability of p-dimethylaminophenylpentazole

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Article information

DOI
https://doi.org/10.1039/C4RA08454C
Article type
Paper
Submitted
21 Aug 2014
Accepted
24 Oct 2014
First published
04 Nov 2014

RSC Adv., 2014,4, 57629-57634

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Thermal stability of p-dimethylaminophenylpentazole

Y. Yang, Y. Li, R. Zhang, C. Sun and S. Pang, RSC Adv., 2014, 4, 57629 DOI: 10.1039/C4RA08454C

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