An atom-economical methodology for the synthesis of sterically hindered tertiary amines was developed, which is based on complementary Rh- and Ru-catalyzed direct reductive amination of ketones with primary and secondary amines using carbon monoxide as a deoxygenating agent.
N. Z. Yagafarov, P. N. Kolesnikov, D. L. Usanov, V. V. Novikov, Y. V. Nelyubina and D. Chusov, Chem. Commun., 2016, 52, 1397 DOI: 10.1039/C5CC08577B
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