First total syntheses of JBIR-04 and unantimycin A have been achieved. Comparison of our spectroscopic data with those reported for natural samples verified the structure of the natural products; (2S,4S,6S,7R,9S,28S) configuration was thus assigned via total synthesis.
Y. Usuki, C. Hamada and T. Satoh, Org. Biomol. Chem., 2017, 15, 7346 DOI: 10.1039/C7OB01732D
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