Preparation of 3D open ordered mesoporous carbon single-crystals and their structural evolution during ammonia activation

Haibo Tan; Jing Tang; Xin Zhou; Dmitri Golberg; Suresh K. Bhatia; Yoshiyuki Sugahara; Yusuke Yamauchi

doi:10.1039/C8CC05318A

Preparation of 3D open ordered mesoporous carbon single-crystals and their structural evolution during ammonia activation†

Haibo Tan,

^ab Jing Tang,*^a Xin Zhou,^ac Dmitri Golberg,^ad Suresh K. Bhatia,

^e Yoshiyuki Sugahara

^b and Yusuke Yamauchi

*^ef

Author affiliations

* Corresponding authors

^a International Center for Materials Nanoarchitectonics (MANA), National Institute for Materials Science (NIMS), 1-1 Namiki, Tsukuba, Ibaraki 305-0044, Japan
E-mail: TANG.Jing@nims.go.jp

^b Faculty of Science and Engineering, Waseda University, 3-4-1 Okubo, Shinjuku, Tokyo 169-8555, Japan

^c Graduate School of Pure and Applied Sciences, University of Tsukuba, Tennodai 1, Tsukuba, Ibaraki 305-8577, Japan

^d School of Chemistry, Physics and Mechanical Engineering, Queensland University of Technology (QUT), 2nd George st., Brisbane, Australia

^e School of Chemical Engineering and Australian, Institute for Bioengineering and Nanotechnology (AIBN), The University of Queensland, Brisbane, QLD 4072, Australia
E-mail: y.yamauchi@uq.edu.au

^f Department of Plant & Environmental New Resources, Kyung Hee University, 1732 Deogyeong-daero, Giheung-gu, Yongin-si, Gyeonggi-do 446-701, South Korea

Abstract

Three-dimensional ordered mesoporous polymer (OMP) single-crystals were synthesized for the first time via a simple soft-template strategy. Ordered mesoporous nitrogen-doped carbon (OMNC) was obtained through carbonization of OMP and post ammonia activation. The evolution of specific surface area, pore volume, and nitrogen content, and species of OMNC were systematically investigated by adjusting the activation temperature and time.

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DOI: https://doi.org/10.1039/C8CC05318A
Article type: Communication
Submitted: 02 Jul 2018
Accepted: 31 Jul 2018
First published: 08 Aug 2018

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Chem. Commun., 2018,54, 9494-9497

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Preparation of 3D open ordered mesoporous carbon single-crystals and their structural evolution during ammonia activation

H. Tan, J. Tang, X. Zhou, D. Golberg, S. K. Bhatia, Y. Sugahara and Y. Yamauchi, Chem. Commun., 2018, 54, 9494 DOI: 10.1039/C8CC05318A

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Chemical Communications

Preparation of 3D open ordered mesoporous carbon single-crystals and their structural evolution during ammonia activation†

Abstract

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Preparation of 3D open ordered mesoporous carbon single-crystals and their structural evolution during ammonia activation

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