Issue 7, 2018
From the journal:

Green Chemistry

Protection of COOH and OH groups in acid, base and salt free reactions†

Xiaotao Zhu,ab   Bo Qian,b   Rongbiao Wei,ab   Jian-Dong Huang ORCID logo a  and  Hongli Bao ORCID logo *b  

* Corresponding authors

a College of Chemistry, Fuzhou University, Fuzhou, Fujian 350108, P. R. China

b State Key Laboratory of Structural Chemistry, Key Laboratory of Coal to Ethylene Glycol and Its Related Technology, Fujian Institute of Research on the Structure of Matter, University of Chinese Academy of Sciences, 155 Yangqiao Road West, Fuzhou, Fujian 350002, P. R. China
E-mail: hlbao@fjirsm.ac.cn

Abstract

We report an iron-catalyzed general functional group protection method with inexpensive reagents. This environmentally benign process does not use acids or bases, and does not produce waste products. Further purification beyond filtration and evaporation is, in most cases, unnecessary. Free COOH and OH groups can be protected in a one-pot reaction.

Graphical abstract: Protection of COOH and OH groups in acid, base and salt free reactions

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Article information

DOI
https://doi.org/10.1039/C8GC00037A
Article type
Communication
Submitted
04 Jan 2018
Accepted
22 Jan 2018
First published
06 Feb 2018

Green Chem., 2018,20, 1444-1447

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Protection of COOH and OH groups in acid, base and salt free reactions

X. Zhu, B. Qian, R. Wei, J. Huang and H. Bao, Green Chem., 2018, 20, 1444 DOI: 10.1039/C8GC00037A

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