Titanium(IV) isopropoxide in ethanol is aged under acidic conditions with a small amount of water. After adding a small amount of N,N-dimethylformamide, TiO2 nanofibers with average diameters of ∼70 nm are prepared by direct electrospinning. During in situ heating of the nanofibers, crystallization into anatase and rutile phases is observed.
B. S. Chapman, S. R. Mishra and J. B. Tracy, Dalton Trans., 2019, 48, 12822 DOI: 10.1039/C9DT01872G
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