Herein, we report a highly selective preparation method of azoxybenzenes from nitrobenzenes by visible-light irradiation. In a batch, this reaction method affords the corresponding aniline derivatives or intermediates (nitrosobenzene or phenyl hydroxylamine); however, in flow microreactors, azoxybenzenes are successfully obtained with very high selectivity.
Y. Nishiyama, A. Fujii and H. Mori, React. Chem. Eng., 2019, 4, 2055 DOI: 10.1039/C9RE00265K
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