A highly efficient Ti-MCM-68 catalyst for phenol oxidation with H2O2 was prepared by a mild liquid-phase treatment for the first time. The key preparation procedures to excellent catalytic activity and high para-selectivity were the use of aqueous solutions of the Ti source and calcination at 650 °C prior to catalytic use.
S. Inagaki, R. Ishizuka, Y. Ikehara, S. Odagawa, K. Asanuma, S. Morimoto and Y. Kubota, RSC Adv., 2021, 11, 3681 DOI: 10.1039/D0RA10081A
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