Accelerating quantitative 13C NMR spectra using an EXtended ACquisition Time (EXACT) method

Zahra H. Al-Aasmi; Alexandra Shchukina; Craig P. Butts

doi:10.1039/D2CC01768G

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Accelerating quantitative ¹³C NMR spectra using an EXtended ACquisition Time (EXACT) method†

Zahra H. Al-Aasmi,

^a Alexandra Shchukina^b and Craig P. Butts

*^a

Author affiliations

* Corresponding authors

^a School of Chemistry, University of Bristol, Cantocks Close, Bristol, UK
E-mail: craig.butts@bristol.ac.uk

^b Faculty of Chemistry, University of Warsaw, Pastera 1, Warsaw, Poland

Abstract

Accurate quantitative ¹³C NMR spectra can be accelerated by using EXACT (EXtended ACquisition Time) NMR methods which reduce Nuclear Overhauser Enhancement (NOE) during the FID. This allows 30–50% shorter experiment times to be used when achieving a given level of quantitative accuracy.

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Article information

DOI: https://doi.org/10.1039/D2CC01768G
Article type: Communication
Submitted: 29 Mar 2022
Accepted: 08 Jun 2022
First published: 08 Jun 2022
This article is Open Access

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Chem. Commun., 2022,58, 7781-7784

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Accelerating quantitative ¹³C NMR spectra using an EXtended ACquisition Time (EXACT) method

Z. H. Al-Aasmi, A. Shchukina and C. P. Butts, Chem. Commun., 2022, 58, 7781 DOI: 10.1039/D2CC01768G

This article is licensed under a Creative Commons Attribution 3.0 Unported Licence. You can use material from this article in other publications without requesting further permissions from the RSC, provided that the correct acknowledgement is given.

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Chemical Communications