Total syntheses of fawcettimine-class Lycopodium alkaloids having an imino bridge between C5 and C13 were accomplished. Fawcettimine was first prepared in 10 steps from a known compound, and the characteristic structures, including the imino bridge, were constructed via the formation of a bridgehead imine.
M. Okuyama, N. Umekubo, K. Akimoto, T. Shimizu, K. Kubokoya, N. Nakajima, Y. Nishiyama and S. Yokoshima, Org. Biomol. Chem., 2023, 21, 6289 DOI: 10.1039/D3OB01065A
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