The use of readily available 1,2,3-thiadiazoles as surrogates of transient alkynyl thiolate anions and diaryliodonium salts as arylating agents allowed for the first time the synthesis of alkynyl aryl sulfides via C(sp2)–S bond formation under transition metal-free conditions.
P. Zaikina, D. Bugaenko and A. Karchava, Org. Biomol. Chem., 2025, Accepted Manuscript , DOI: 10.1039/D5OB00576K
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