Catalysed reduction of diol thiocarbonates with tributyltin hydride followed by appropriate alkaline hydrolysis affords a convenient synthesis of 2-, 3-, 4-, and 5-deoxysugars and of 2′- and 3′-deoxynucleosides.
D. H. R. Barton and R. Subramanian, J. Chem. Soc., Chem. Commun., 1976, 867 DOI: 10.1039/C39760000867
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