Reaction of N[(CH2)2As(C6H5)2]3(1) with gaseous HI leads to{HN[(CH2)2Asl2]3}I2(2) and hydrolysis of (2) with H2O–NH3 in tetrahydrofuran gives [N(CH2CH2)3]8(As4O4)6(3); single crystal X-ray diffraction shows that one moleculer of (3) contains six eight-membereds As4O4ring connected together by triethylamine units.
J. Ellermann, A. Veit, E. Lindner and S. Hoehne, J. Chem. Soc., Chem. Commun., 1982, 382 DOI: 10.1039/C39820000382
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