Two polymorphs of 2,6-di-tert-butylnaphthalene, which differ by a factor of twelve in the number of crystallographically independent tert-butyl group environments, have been characterized by a synergistic combination of low-frequency 1H NMR spin–lattice relaxation rate measurements and conventional crystallographic structure determinations.
Superlattices, polymorphs and solid-state NMR spin–lattice relaxation (T1) measurements of 2,6-di-tert-butylnaphthalene
A. L. Rheingold, J. S. Figueroa, C. Dybowski and P. A. Beckmann, Chem. Commun., 2000, 651 DOI: 10.1039/A909449K
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