Issue 81, 2013
From the journal:

Chemical Communications

Single source precursor routes for synthesis of PdTe nanorods and particles: solvent dependent control of shapes†

Kamal Nayan Sharma,a   Hemant Joshi,a   Alpesh K. Sharma,a   Om Prakasha  and  Ajai K. Singh*a  

* Corresponding authors

a Department of Chemistry, Indian Institute of Technology Delhi, New Delhi 110016, India
E-mail: aksingh@chemistry.iitd.ac.in, ajai57@hotmail.com
Fax: +91-01-26581102
Tel: +91-011-26591379

Abstract

The PdTe NPs (hexagonal) and nanorods (first example) have been synthesized for the first time from single source precursors (SSPs), [Pd(L1)Cl2] (1) and [Pd(L2)Cl]BF4 (2) [L1, 4-bromo-1-[2-(4-methoxyphenyltellanyl)ethyl]-1H-pyrazole; L2, bis-[2-(4-bromopyrazol-1-yl)ethyl]telluride], by their thermolysis in an OA–ODE mixture (1 : 1) and TOP respectively. The composition of the PdTe phase does not change with SSP/solvent. Complex 2 gives small size nanostructures.

Graphical abstract: Single source precursor routes for synthesis of PdTe nanorods and particles: solvent dependent control of shapes

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Article information

DOI
https://doi.org/10.1039/C3CC45175E
Article type
Communication
Submitted
10 Jul 2013
Accepted
12 Aug 2013
First published
12 Aug 2013

Chem. Commun., 2013,49, 9344-9346

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Single source precursor routes for synthesis of PdTe nanorods and particles: solvent dependent control of shapes

K. N. Sharma, H. Joshi, A. K. Sharma, O. Prakash and A. K. Singh, Chem. Commun., 2013, 49, 9344 DOI: 10.1039/C3CC45175E

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