Gold-catalyzed aerobic oxygenative cleavage of triple bonds that occurs under the ambient pressure of air and at room temperature is reported; radical inhibition tests suggest that oxygenation occurs via a gold-bound metalloradical intermediate.
D. V. Patil, H. Park, J. Koo, J. W. Han and S. Shin, Chem. Commun., 2014, 50, 12722 DOI: 10.1039/C4CC04153D
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