Mechanochemical synthesis has been applied to the rapid synthesis of Deep Eutectic Solvents (DESs), including Reline 200 (choline chloride : urea, 1 : 2), in a continuous flow methodology by Twin Screw Extrusion (TSE). This gave products in higher purity and with Space Time Yields (STYs), four orders of magnitude greater than for batch methods.
D. E. Crawford, L. A. Wright, S. L. James and A. P. Abbott, Chem. Commun., 2016, 52, 4215 DOI: 10.1039/C5CC09685E
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