Issue 104, 2016, Issue in Progress
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RSC Advances

Quantitative 13C NMR characterization of fast pyrolysis oils

R. M. Happs,a   K. Iisa ORCID logo a  and  J. R. Ferrell III*a  

* Corresponding authors

a National Bioenergy Center, National Renewable Energy Laboratory, Golden, CO, USA
E-mail: jack.ferrell@nrel.gov

Abstract

Quantitative 13C NMR analysis of model catalytic fast pyrolysis (CFP) oils following literature procedures showed poor agreement for aromatic hydrocarbons between NMR measured concentrations and actual composition. Modifying integration regions based on DEPT analysis for aromatic carbons resulted in better agreement. Solvent effects were also investigated for hydrotreated CFP oil.

Graphical abstract: Quantitative 13C NMR characterization of fast pyrolysis oils

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Article information

DOI
https://doi.org/10.1039/C6RA24044E
Article type
Communication
Submitted
27 Sep 2016
Accepted
20 Oct 2016
First published
20 Oct 2016

RSC Adv., 2016,6, 102665-102670

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Quantitative 13C NMR characterization of fast pyrolysis oils

R. M. Happs, K. Iisa and J. R. Ferrell III, RSC Adv., 2016, 6, 102665 DOI: 10.1039/C6RA24044E

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